A basis for the space of functions analytic in a disk by Nagnibida N. I.

By Nagnibida N. I.

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Monotropic substances are characterized by the existence of a purely hypothetical transition point, since this point is predicted to be higher in temperature than the melting point of one of the polymorphic forms. 108 Scanning electron microscopy (SEM) is the technique of choice when one seeks to obtain information at high-magnification levels, or when a three-dimensional view of a particle surface is required. A conventional SEM is similar to an inverted light microscopy, in that the source lies above the specimen, the interrogating electron beam focused by a series of lenses, and the image constructed on the basis of scattered electromagnetic radiation.

Studies of the desolvation of solvatomorphs can be conducted using VT-XRPD. For instance, after the dehydration of a hydrate phase, one may obtain either a crystalline anhydrate phase or an amorphous phase and the XRPD pattern will clearly indicate the difference. In addition, should one encounter an equivalence in powder patterns between the hydrate phase and its dehydrated form, this would indicate the existence of channel-type water (as opposed to lattice bound water). 141,142 VT-XRPD has been used to study the desolvation and ultimate decomposition of the various hydrates.

Thermal Methods of Analysis Thermal methods of analysis can be defined as those techniques in which a property of the substance under study is determined as a function of an externally applied and programmed temperature. , crystallization and oxidative decomposition). 153–157 Significant insight into the practice of thermal analysis can be gleaned from a consideration of the determination of ordinary melting points through study of fusion curves, for which a typical example is provided in Figure 7.

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